Distillation Labware
Glassware and replacement parts designed to carry out distillations in laboratory settings; includes condensers, distillation heads, receivers, etc. Products are available for various scales and for specialty distillations.
Distillation is a process used widely in the laboratory or in wider working environments for separating or purifying liquids or liquid mixtures based on the different boiling points of individual components.
Distillation Applications:
• Separation and purification of miscible liquid mixtures in organic chemistry
• Drying of solid residues and/or solvent removal
• Fractional distillation of liquids from polymers and petroleum products
• Removal of particulates or other solid contaminants
• As part of a water purification system for production of distilled water for laboratory use
• Specialist steam distillation-based applications such as Kjeldahl analysis of nitrogen and proteins in food, beverage, or environmental samples
What Types of Distillation Equipment Are Available?
Conventional distillation apparatus, typically comprising individual, jointed borosilicate glassware components assembled by the user (depending upon the application), using appropriate clamps, stands, and supports. Most conventional distillation assemblies combine a round-bottomed distilling flask to contain and heat the liquid(s) that require purification, fitted with a stoppered or jointed neck to which is attached a downward-sloping, inclined side-arm for connection to a condensing unit to cool the heated vapors back down to their liquid state. Heating mantles are the preferred heat source for improved temperature control. These conventional distillation units are also available supplied complete and ready-assembled for added convenience and ease of use.
Specialized automated distillation equipment, notably units designed for the determination of volatile acidity and alcoholic strength by volume in wines, musts, and alcoholic beverages, and units designed for Kjeldahl nitrogen or protein determinations.
Ace Glass, Inc. 24/40 25mL Dean & Stark Moisture Test Receiver
24/40 25mL Dean & Stark Moisture Test Receiver with return line to allow excess solvent to return to the boiling flask. Suitable for ASTM D 95 and E 123.
Ace Glass, Inc. 10mL 24/40 Barrett moisture test receiver, jacketed sidearm, glass plug
10mL Barrett type moisture test receiver with 24/40 standard taper joints for use in determining the water content in petroleum and bituminous material. Features a jacketed side arm and is supplied with 2mm bore glass plug.
Ace Glass, Inc. Splitter, distillation, reflux, 45/50 top & bottom joints, 0-10mmside valve, 1/2-in ground outlet
Splitter, distillation, reflux, 45/50 top & bottom joints, 0-10mmside valve, 1/2-in ground outlet
Ace Glass, Inc. 24/40 250mL distillation receiver
250mL borosilicate glass jacketed distilling receiver with 24/40 joint has vacuum manifold for removal of the sample during operation, without disturbing the system. Manifold stopcocks are 4mm bore, and receiver stopcock is 3mm bore. Condenser hose connections are size E, for use with 9.5mm (3/8) or 11.1mm (7/16) I.D. tubing. Manifold has 10mm O.D. olive-style connections.
Ace Glass, Inc. 24/40 50.8cm distillation column
50.8cm Hemple distillation column with 24/40 standard taper joints, and indentations to support packing. Length in centimeters refers to the length from the packing support to the bottom of the outer ground joint.
Ace Glass, Inc. 12 SECTION SNYDER COLUMN 12 SECTION SNYDER COLUMN
12-section Snyder column for use in distillation applications. Column is floating ball type with 24/40 joints. Each section is approximately 51mm long.
Ace Glass, Inc. Splitter, distillation, reflux, 24/40 top & bottom joints, 0-10mmside valve, 1/2-in ground outlet
Splitter, distillation, reflux, 24/40 top & bottom joints, 0-10mmside valve, 1/2-in ground outlet
Ace Glass, Inc. 24/40 variable reflux ratio distilling head with 10/30 thermometer joint
24/40 variable reflux ratio distilling head with 10/30 thermometer joint takes 76mm immersion thermometers. Side arm joint is 24/40. Head is constructed so that satisfactory operation can be maintained under any pressure condition.
Ace Glass, Inc. Still, solvent recovery, complete, includes adapter and condenser
Still, solvent recovery, complete, includes adapter and condenser
Chemglass Life Sciences 150mL HW Pressure Vessel, Round Bottom, #25 Internal Thread, Vessel Only, 63.5mm O.D. x 117mm Length, Bushing Size/25
150mL HW Pressure Vessel, Round Bottom, #25 Internal Thread, Vessel Only, 63.5mm O.D. x 117mm Length, Bushing Size/25. Heavy wall pressure vessels have an internal thread for use with PTFE bushings as pressure seals. The design allows hand tightening/loosening for easy access into the vessel. O-ring is positioned on the bushing above the thread for improved sealing. Supplied complete with vessel, PTFE bushing & Viton o-ring. Optional Perfluoro o-ring has the chemical resistance & service temperature range similar to Kalrez 4079. See CG-362, CG-364, and CG-366 for optional PTFE Bushings.IMPORTANT NOTICE: ALL CHEMGLASS PRESSURE VESSELS ARE TESTED AT 150 PSI, OR APPROX TWO AND ONE-HALF TIMES THEIR RECOMMENDED WORKING PRESSURE. HOWEVER, CHEMGLASS DOES NOT GUARANTEE THE VESSEL FROM BREAKING UNDER PRESSURE, DUE TO THE NATURE OF MATERIAL AND CONDITIONS BEYOND OUR CONTROL. CHEMGLASS RECOMMENDS THE USE OF SAFETY SHIELDS AND/OR OTHER SAFETY EQUIPMENT.
Chemglass Life Sciences 150mL Heavy Wall Pressure Vessel, Round Bottom, #15 Internal Thread, Vessel Only, 63.5mm O.D. x 117mm Length, Bushing Size/15
150mL Heavy Wall Pressure Vessel, Round Bottom, #15 Internal Thread, Vessel Only, 63.5mm O.D. x 117mm Length, Bushing Size/15. Heavy wall pressure vessels have an internal thread for use with PTFE bushings as pressure seals. The design allows hand tightening/loosening for easy access into the vessel. O-ring is positioned on the bushing above the thread for improved sealing. Supplied complete with vessel, PTFE bushing & Viton o-ring. Optional Perfluoro o-ring has the chemical resistance & service temperature range similar to Kalrez 4079. See CG-362, CG-364, and CG-366 for optional PTFE Bushings.IMPORTANT NOTICE: ALL CHEMGLASS PRESSURE VESSELS ARE TESTED AT 150 PSI, OR APPROX TWO AND ONE-HALF TIMES THEIR RECOMMENDED WORKING PRESSURE. HOWEVER, CHEMGLASS DOES NOT GUARANTEE THE VESSEL FROM BREAKING UNDER PRESSURE, DUE TO THE NATURE OF MATERIAL AND CONDITIONS BEYOND OUR CONTROL. CHEMGLASS RECOMMENDS THE USE OF SAFETY SHIELDS AND/OR OTHER SAFETY EQUIPMENT.
Chemglass Life Sciences 48mL Heavy Wall Pressure Vessel, Cylindrical, #15 Internal Thread, Complete, 38mm O.D. x 114mm Length, Bushing Size/15
48mL Heavy Wall Pressure Vessel, Cylindrical, #15 Internal Thread, Complete, 38mm O.D. x 114mm Length, Bushing Size/15. Heavy wall pressure vessels have an internal thread for use with PTFE bushings as pressure seals. The design allows hand tightening/loosening for easy access into the vessel. O-ring is positioned on the bushing above the thread for improved sealing. Supplied complete with vessel, PTFE bushing & Viton o-ring. Optional Perfluoro o-ring has the chemical resistance & service temperature range similar to Kalrez 4079. See CG-362, CG-364, and CG-366 for optional PTFE Bushings.IMPORTANT NOTICE: ALL CHEMGLASS PRESSURE VESSELS ARE TESTED AT 150 PSI, OR APPROX TWO AND ONE-HALF TIMES THEIR RECOMMENDED WORKING PRESSURE. HOWEVER, CHEMGLASS DOES NOT GUARANTEE THE VESSEL FROM BREAKING UNDER PRESSURE, DUE TO THE NATURE OF MATERIAL AND CONDITIONS BEYOND OUR CONTROL. CHEMGLASS RECOMMENDS THE USE OF SAFETY SHIELDS AND/OR OTHER SAFETY EQUIPMENT.